Determination of The Concentration of Chemical Elements in The Walnut Septum Using Inductively Coupled Plasma Optical Emission Spectrometry

Authors

  • Asqarov Ibrohim Rahmonovich Doctor of Chemical Sciences, Professor, Department of Chemistry, Andijan State University, Andijan, Uzbekistan
  • Mamatokhtayeva Dilnoza Dilshodbek kizi Master’s Student in Chemistry, Andijan State University, Andijan, Uzbekistan

DOI:

https://doi.org/10.37547/ijasr-06-04-05

Keywords:

Walnut fruit septum, micro-elements and macro-elements, ICP-OES method

Abstract

This article provides a comprehensive investigation into the chemical composition of the walnut (Juglans regia L.) fruit septum, specifically focusing on the methodologies for preparing dry ash mass from the laminae and the subsequent extraction processes from the resulting ash. The analytical study was conducted using Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES), which enabled the screening of 68 distinct chemical elements. The findings reveal that among the elements analysed, 35 chemical elements exhibited concentrations exceeding the Limit of Detection (<LOD). Notably, five specific macro-elements were identified in substantial quantities, demonstrating an increasing concentration gradient in the order of Na < P < Mg < K < Ca. Given that the walnut septum is exceptionally rich in these 35 macro- and micro-elements, the study provides strategic recommendations for its utilisation as an effective and promising raw material in the pharmaceutical industry, particularly for the development and production of therapeutic food supplements and nutraceuticals.

References

1. Berzegova, A. A. (2007). Химический состав плодов грецкого ореха. Новые технологии, (4), 42–43.

2. Vasipov, V. V., & Vytovtov, A. A. (2016). Грецкий орех (Juglans regia L.) – перспективный источник биологически активных веществ. In Пища. Экология. Качество: Труды XIII международной научно-практической конференции (pp. 223–228).

3. Ivanova, R. A., & Elisovetskaya, D. S. (2014). Антиоксидантная активность экстрактов из различных видов незрелых орехов Juglans spp. In Лекарственные растения: биоразнообразие, технологии, применение (pp. 129–131). ГГАУ.

4. Karomatov, I. D. (2012). Простые лекарственные средства. Бухара.

5. Makarenkova, O. G., Shevyakova, L. V., & Bessonov, V. V. (2016). Природные микроэлементы орехов – неотъемлемая часть здорового питания. Вопросы питания, 85(2), 202.

6. Ostrikov, A. N., Gorbatova, A. V., & Filiptsov, P. V. (2016). Анализ жирнокислотного состава масел арахиса и грецкого ореха. Технологии пищевой и перерабатывающей промышленности АПК, 4(12), 37–42.

7. Khayrieva, M. F., & Karomatov, I. D. (2018). Грецкий орех и метаболические нарушения (обзор литературы). Биология и интегративная медицина, (8), 25.

8. Abdallah, I. B., Tlili, N., Martinez-Force, E., Rubio, A. G., Perez-Camino, M. C., Albouchi, A., & Boukhchina, S. (2015). Content of carotenoids, tocopherols, sterols, triterpenic and aliphatic alcohols, and volatile compounds in six walnuts (Juglans regia L.) varieties. Food Chemistry, 173, 972–978. https://doi.org/10.1016/j.foodchem.2014.10.095

9. Gutiérrez Ortiz, A. L., Berti, F., Navarini, L., Crisafulli, P., Colomban, S., & Forzato, C. (2018). Aqueous extracts of walnut (Juglans regia L.) leaves: Quantitative analyses of hydroxycinnamic and chlorogenic acids. Journal of Chromatographic Science, 56(8), 753–760. https://doi.org/10.1093/chromsci/bmy041

10. Li, Q., Deng, A. J., Li, L., Wu, L. Q., Ji, M., Zhang, H. J., Li, Z. H., Ma, L., Zhang, Z. H., Chen, X. G., & Qin, H. L. (2017). Azacyclo-indoles and phenolics from the flowers of Juglans regia. Journal of Natural Products, 80(8), 2189–2198. https://doi.org/10.1021/acs.jnatprod.6b00887

11. Liu, C., Tai, Z., Feng, S., Fang, Y., Cai, L., & Ding, Z. (2012). Chemical constituents from the seed coat of Juglans regia. Zhongguo Zhong Yao Za Zhi, 37(10), 1417–1421.

12. Luo, J. J., Yang, B., Zeng, Y., & Li, C. (2012). Chemical constituents from the flower of Juglans regia. Zhong Yao Cai, 35(10), 1614–1616.

13. Paudel, P., Satyal, P., Dosoky, N. S., Maharjan, S., & Setzer, W. N. (2013). Juglans regia and J. nigra, two trees important in traditional medicine: A comparison of leaf essential oil compositions and biological activities. Natural Product Communications, 8(10), 1481–1486.

14. Rather, M. A., Dar, B. A., Dar, M. Y., Wani, B. A., Shah, W. A., Bhat, B. A., Ganai, B. A., Bhat, K. A., Anand, R., & Qurishi, M. A. (2012). Chemical composition, antioxidant and antibacterial activities of the leaf essential oil of Juglans regia L. Phytomedicine, 19(13), 1185–1190. https://doi.org/10.1016/j.phymed.2012.07.018

15. Schwindl, S., Kraus, B., & Heilmann, J. (2017). Phytochemical study of Juglans regia L. leaves. Phytochemistry, 144, 58–70. https://doi.org/10.1016/j.phytochem.2017.08.012

16. Tsasi, G., Milošević-Ifantis, T., & Skaltsa, H. (2016). Phytochemical study of Juglans regia L. pericarps from Greece with a chemotaxonomic approach. Chemistry & Biodiversity, 13(12), 1636–1640. https://doi.org/10.1002/cbdv.201600067

17. Wang, D., Mu, Y., Dong, H., Yan, H., Hao, C., Wang, X., & Zhang, L. (2018). Chemical constituents of the ethyl acetate extract from Diaphragma juglandis fructus and their inhibitory activity on nitric oxide production in vitro. Molecules, 23(1), Article E72. https://doi.org/10.3390/molecules23010072

18. Zhao, M. H., Jiang, Z. T., Liu, T., & Li, R. (2014). Flavonoids in Juglans regia L. leaves and evaluation of in vitro antioxidant activity via intracellular and chemical methods. The Scientific World Journal, 2014, Article 303878. https://doi.org/10.1155/2014/303878

19. Litvinsky, V. A., Grishina, E. A., Nosikov, V. V., & Sushkova, L. O. (2018). Атомно-эмиссионная спектроскопия с индуктивно связанной плазмой для определения содержания меди в растениях и продукции растениеводства. Плодородие, (5). https://doi.org/10.25680/S19948603.2018.104.18

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Published

2026-04-20

How to Cite

Asqarov Ibrohim Rahmonovich, & Mamatokhtayeva Dilnoza Dilshodbek kizi. (2026). Determination of The Concentration of Chemical Elements in The Walnut Septum Using Inductively Coupled Plasma Optical Emission Spectrometry. International Journal of Advance Scientific Research, 6(04), 56-63. https://doi.org/10.37547/ijasr-06-04-05

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